國家衛生研究院 NHRI:Item 3990099045/6478
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    题名: Palladium(II) acetate mediated oxidative cyclization of omega-unsaturated alpha-cyano ketones for facile construction of methylenecyclohexane ring system
    其它题名: Palladium(II) acetate mediated oxidative cyclization of ω-unsaturated α-cyano ketones for facile construction of methylenecyclohexane ring system
    作者: Hsieh, MT;Shia, KS;Liu, HJ;Kuo, SC
    贡献者: Institute of Biotechnology and Pharmaceutical Research
    摘要: A highly efficient annulative approach towards the construction of the structurally attractive methylenecyclohexane ring was developed through a convenient 1,4-addition of 4-pentenylmagnesium bromide to 2-cyano-2-cycloalkenones followed by a Pd( II )-mediated oxidative cyclization of the resulting ω -unsaturated α -cyano ketones. Based on this newly developed protocol, polycyclic adducts bearing various ring sizes and substitutions can be prepared in moderate to high yields.
    日期: 2012-05
    關聯: Organic & Biomolecular Chemistry. 2012 May;10(23):4609-4617.
    Link to: http://dx.doi.org/10.1039/C2OB25161B
    JIF/Ranking 2023: http://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=NHRI&SrcApp=NHRI_IR&KeyISSN=1477-0520&DestApp=IC2JCR
    Cited Times(WOS): https://www.webofscience.com/wos/woscc/full-record/WOS:000304352000019
    Cited Times(Scopus): http://www.scopus.com/inward/record.url?partnerID=HzOxMe3b&scp=84862239255
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